This is the RMarkdown file for the FTICR results from the 3Soils experiment. Tables and figures for molecular results.

Run: 2020-04-21

Color palette used: treatments == viridis | | | | |—–|—–|—–| |field moist | #35b779ff| green | |drought |#fde725ff | yellow | |flood | #443a83ff | blue |

FTICR domains

domains with NOSC

FTICR Pores – figures

native SOM

treatment effect – all peaks

treatment effect – unique peaks

unique in each treatment compared to all, including TZflood these are peaks that were uniquely added during a given treatment

peaks lost and gained

treatment effect – relative abundance

Relative abundance

Relative abundance

treatment effect – NOSC

NOSC for CPCRW

NOSC for CPCRW

NOSC table

tension site drought field moist flood time zero saturation
1.5 kPa Alaska -0.4615 -0.4545 -0.6207 -0.5217
1.5 kPa Florida -0.5714 -0.4000 -0.4000 -0.4000
1.5 kPa Washington -0.7333 -0.7586 -0.6000 -0.7500
50 kPa Alaska -0.3750 -0.3077 -0.4615 -0.3333
50 kPa Florida -0.4828 -0.3478 -0.3333 -0.3636
50 kPa Washington -0.6250 -0.6667 -0.7826 -0.5578

aromatic peaks

not doing much with aromatic peaks, because it excludes many lignins and tannins that contain aromatic groups

shannon diversity index –

aromatic peaks

aromatic peaks

FTICR Pores – tables

peaks

#> [1] "50 kPa"
site Class drought field moist flood time zero saturation
Alaska AminoSugar 201 5 17 10
Alaska Carb 255 7 51 15
Alaska Lipid 148 38 152 120
Alaska Protein 511 79 352 180
Alaska UnsatHC 2 8 1 9
Alaska ConHC 138 136 150 247
Alaska Lignin 1391 1001 1168 1230
Alaska Tannin 229 93 118 120
Alaska Other 11 8 1 10
Alaska total 2886 1375 2010 1941
Florida AminoSugar 34 18 23 254
Florida Carb 68 2 24 273
Florida Lipid 132 54 103 146
Florida Protein 416 188 250 535
Florida UnsatHC 4 3 8 15
Florida ConHC 105 132 194 144
Florida Lignin 1062 996 1072 1243
Florida Tannin 78 105 150 187
Florida Other 10 1 2 20
Florida total 1909 1499 1826 2817
Washington AminoSugar 6 26 57 34
Washington Carb 5 18 11 2
Washington Lipid 133 176 228 108
Washington Protein 245 250 490 283
Washington UnsatHC 3 15 15 16
Washington ConHC 3 13 15 61
Washington Lignin 593 741 738 776
Washington Tannin 4 11 10 30
Washington Other 1 4 4 2
Washington total 993 1254 1568 1312
#> [1] "1.5 kPa"
site Class drought field moist flood time zero saturation
Alaska AminoSugar 129 13 21 36
Alaska Carb 181 22 27 15
Alaska Lipid 98 122 204 142
Alaska Protein 395 270 431 446
Alaska UnsatHC 3 15 13 14
Alaska ConHC 53 142 95 171
Alaska Lignin 854 1034 1029 981
Alaska Tannin 98 92 62 92
Alaska Other 27 8 10 6
Alaska total 1838 1718 1892 1903
Florida AminoSugar 25 20 2 265
Florida Carb 75 6 12 310
Florida Lipid 114 106 70 122
Florida Protein 324 248 143 511
Florida UnsatHC 4 8 6 12
Florida ConHC 35 152 151 55
Florida Lignin 778 1029 744 900
Florida Tannin 18 97 41 138
Florida Other 14 6 2 29
Florida total 1387 1672 1171 2342
Washington AminoSugar 20 53 16 45
Washington Carb 3 23 8 9
Washington Lipid 188 168 106 135
Washington Protein 301 428 115 376
Washington UnsatHC 11 11 19 17
Washington ConHC 25 13 26 32
Washington Lignin 581 617 518 531
Washington Tannin 11 10 10 9
Washington Other 3 5 NA 3
Washington total 1143 1328 818 1157

unique peaks

#> [1] "50 kPa"
site Class drought field moist flood
Alaska AminoSugar 185 NA 2
Alaska Carb 202 1 NA
Alaska Lipid 20 1 20
Alaska Protein 182 NA 21
Alaska UnsatHC NA 2 NA
Alaska ConHC 5 4 4
Alaska Lignin 214 9 23
Alaska Tannin 99 NA 5
Alaska Other 7 NA NA
Florida AminoSugar 4 2 2
Florida Carb 6 NA NA
Florida Lipid 20 NA 10
Florida Protein 68 7 4
Florida UnsatHC NA NA 2
Florida ConHC 6 5 57
Florida Lignin 26 13 34
Florida Tannin 1 2 32
Florida Other 4 NA NA
Washington AminoSugar NA 10 19
Washington Carb 2 9 1
Washington Lipid 28 11 57
Washington Protein 9 12 116
Washington UnsatHC NA 1 2
Washington ConHC NA NA 3
Washington Lignin 2 14 64
Washington Tannin NA NA 3
Washington Other NA 2 2
#> [1] "1.5 kPa"
site Class drought field moist flood
Alaska AminoSugar 108 NA 2
Alaska Carb 160 4 3
Alaska Lipid 8 5 65
Alaska Protein 71 4 42
Alaska UnsatHC NA 7 3
Alaska ConHC 5 3 3
Alaska Lignin 67 42 74
Alaska Tannin 15 5 NA
Alaska Other 17 NA NA
Florida AminoSugar 7 6 NA
Florida Carb 5 NA NA
Florida Lipid 23 11 3
Florida Protein 37 9 NA
Florida UnsatHC NA 4 2
Florida ConHC 4 29 26
Florida Lignin 21 122 2
Florida Tannin 1 34 NA
Florida Other 6 4 NA
Washington AminoSugar NA 11 3
Washington Carb NA 15 1
Washington Lipid 51 16 3
Washington Protein 20 70 8
Washington UnsatHC NA NA 4
Washington ConHC 7 10 8
Washington Lignin 49 82 18
Washington Tannin 4 5 1
Washington Other 1 4 NA

relative abundance

#> [1] "50 kPa"
site Class drought field moist flood time zero saturation
Alaska AminoSugar 5.8 ± 0.74 * 0.36 ± 0 0.77 ± 0.08 0.47 ± 0.06
Alaska Carb 7.97 ± 0.58 * 0.51 ± 0 1.99 ± 0.65 0.51 ± 0.17
Alaska Lipid 5.33 ± 0.33 2.76 ± 0 * 7.37 ± 0.26 * 5.53 ± 0.51
Alaska Protein 18.01 ± 0.67 * 5.75 ± 0 * 17.37 ± 0.31 * 8.73 ± 0.69
Alaska UnsatHC 0.06 ± 0.01 * 0.58 ± 0 * 0.05 ± 0 * 0.38 ± 0.07
Alaska ConHC 4.62 ± 0.38 * 9.89 ± 0 7.26 ± 0.46 * 11.07 ± 1.54
Alaska Lignin 50.28 ± 0.82 * 72.8 ± 0 * 59.32 ± 0.71 * 66.41 ± 1.05
Alaska Tannin 7.56 ± 0.56 6.76 ± 0 5.84 ± 0.04 6.56 ± 0.26
Alaska Other 0.37 ± 0.02 0.58 ± 0 0.05 ± 0 0.42 ± 0.12
Florida AminoSugar 1.62 ± 0.16 * 1.2 ± 0 * 1.09 ± 0.14 * 8.52 ± 0.81
Florida Carb 3.4 ± 0.23 * 0.13 ± 0 * 1.26 ± 0.18 * 9.37 ± 0.71
Florida Lipid 6.72 ± 0.19 3.6 ± 0 4.98 ± 0.68 4.95 ± 0.6
Florida Protein 21.71 ± 0.48 12.54 ± 0 * 13.29 ± 1.35 * 18.81 ± 0.33
Florida UnsatHC 0.19 ± 0.02 * 0.2 ± 0 * 0.38 ± 0.07 0.51 ± 0.03
Florida ConHC 5.07 ± 0.56 8.81 ± 0 * 10.45 ± 0.72 * 4.87 ± 0.31
Florida Lignin 56.83 ± 0.32 * 66.44 ± 0 * 60.45 ± 1.67 * 45.65 ± 1.16
Florida Tannin 3.95 ± 0.14 7 ± 0 8 ± 1.2 6.58 ± 0.05
Florida Other 0.51 ± 0.02 0.07 ± 0 0.12 ± 0.01 0.73 ± 0.03
Washington AminoSugar 0.5 ± 0.11 * 2.09 ± 0.11 3.4 ± 0.12 * 2.13 ± 0.57
Washington Carb 0.51 ± 0 * 1.11 ± 0.14 * 0.61 ± 0.03 * 0.14 ± 0.03
Washington Lipid 11.51 ± 1.93 13.35 ± 0.52 * 14.41 ± 0.54 * 8.19 ± 1.01
Washington Protein 21.26 ± 3.68 18.53 ± 1.62 31.9 ± 0.27 * 20.61 ± 2.69
Washington UnsatHC 0.25 ± 0.03 * 1.21 ± 0.06 0.91 ± 0.08 1.1 ± 0.23
Washington ConHC 0.32 ± 0.01 * 0.93 ± 0.06 * 0.96 ± 0.03 * 3.95 ± 1.08
Washington Lignin 65.32 ± 5.84 61.8 ± 1.77 47.02 ± 0.7 * 61.77 ± 3.38
Washington Tannin 0.37 ± 0.03 * 0.72 ± 0.14 * 0.56 ± 0.1 * 1.99 ± 0.4
Washington Other 0.13 ± 0.02 0.25 ± 0.04 0.22 ± 0.05 0.16 ± 0.02

total = 100%

#> [1] "1.5 kPa"
site Class drought field moist flood time zero saturation
Alaska AminoSugar 6.03 ± 0.61 * 0.65 ± 0.06 0.94 ± 0.13 1.72 ± 0.17
Alaska Carb 9.1 ± 0.74 * 0.84 ± 0.28 1.18 ± 0.17 0.7 ± 0.09
Alaska Lipid 5.37 ± 0.19 * 7.27 ± 0.43 10.88 ± 0.46 * 7.73 ± 0.59
Alaska Protein 22.43 ± 1.1 17.16 ± 1.35 23.04 ± 0.78 22.04 ± 2.32
Alaska UnsatHC 0.14 ± 0.03 * 0.67 ± 0.11 0.64 ± 0.02 0.62 ± 0.07
Alaska ConHC 2.59 ± 0.4 * 7.63 ± 0.58 4.32 ± 0.86 6.64 ± 1.87
Alaska Lignin 48.02 ± 0.81 * 60.41 ± 0.94 * 55.51 ± 0.12 55.57 ± 1.94
Alaska Tannin 5.04 ± 0.5 5.07 ± 0.24 3.08 ± 0.33 * 4.77 ± 0.31
Alaska Other 1.3 ± 0.08 0.38 ± 0.09 0.41 ± 0.08 0.27 ± 0.07
Florida AminoSugar 1.55 ± 0.16 * 1.07 ± 0.2 * 0.16 ± 0.02 * 8.94 ± 1.55
Florida Carb 5.48 ± 0.43 * 0.34 ± 0.03 * 0.86 ± 0.3 * 10.87 ± 2.15
Florida Lipid 8.11 ± 0.64 6.16 ± 0.21 6.33 ± 0.86 7.45 ± 2.43
Florida Protein 24.08 ± 0.89 14.32 ± 1.25 * 12.03 ± 1.3 * 26.79 ± 4.57
Florida UnsatHC 0.27 ± 0.04 * 0.41 ± 0.09 0.53 ± 0.08 0.59 ± 0.09
Florida ConHC 1.94 ± 0.37 7.93 ± 1.55 * 12.15 ± 1.42 * 1.9 ± 0.33
Florida Lignin 56.59 ± 1.27 * 63.53 ± 1.02 * 64.52 ± 1.7 * 38.04 ± 2.26
Florida Tannin 0.99 ± 0.16 * 5.93 ± 0.17 3.24 ± 0.28 4.41 ± 1.19
Florida Other 0.97 ± 0.03 0.32 ± 0.04 0.17 ± 0.04 1.01 ± 0.2
Washington AminoSugar 1.31 ± 0.36 * 3.68 ± 0.46 1.87 ± 0.17 * 3.73 ± 0.16
Washington Carb 0.25 ± 0.04 1.69 ± 0.44 * 0.89 ± 0.08 0.7 ± 0.04
Washington Lipid 16.86 ± 0.61 * 12.43 ± 0.25 12.89 ± 0.29 11.64 ± 0.14
Washington Protein 21.9 ± 3.95 * 30.01 ± 3.06 13.45 ± 0.64 * 33.57 ± 0.94
Washington UnsatHC 1.11 ± 0.21 0.9 ± 0.15 * 2.21 ± 0.07 * 1.47 ± 0.02
Washington ConHC 1.77 ± 0.58 0.91 ± 0.13 2.68 ± 0.67 2.56 ± 0.38
Washington Lignin 55.8 ± 4.48 49.36 ± 2.11 64.99 ± 0.75 * 45.26 ± 1.34
Washington Tannin 1.18 ± 0.21 0.69 ± 0.17 1.02 ± 0.13 0.8 ± 0.09
Washington Other 0.34 ± 0.14 0.34 ± 0.07 NA 0.27 ± 0.04

total = 100% ## aromatic peaks

Shannon diversity

treatment 1.5 kPa Alaska 1.5 kPa Florida 1.5 kPa Washington 50 kPa Alaska 50 kPa Florida 50 kPa Washington
drought 1.53 ± 0.01 * 1.27 ± 0.02 * 1.17 ± 0.07 * 1.53 ± 0.02 * 1.33 ± 0.01 * 0.94 ± 0.1
field moist 1.26 ± 0.02 1.21 ± 0.03 * 1.28 ± 0.02 1.01 ± 0 * 1.13 ± 0 * 1.15 ± 0.02
flood 1.29 ± 0.02 1.16 ± 0.04 * 1.15 ± 0.03 * 1.28 ± 0.03 * 1.28 ± 0.04 * 1.27 ± 0.01
time zero saturation 1.31 ± 0.04 1.6 ± 0.06 1.34 ± 0.01 1.15 ± 0.03 1.64 ± 0.02 1.15 ± 0.07

FTICR Soil – figures

native SOM

treatment effect – all peaks

treatment effect – unique peaks

peaks lost and gained

treatment effect – relative abundance

NOSC

NOSC table

site baseline drought field moist flood time zero saturation
Alaska -0.3636 -0.3529 -0.3846 -0.4211 -0.4000
Florida -0.3200 -0.4545 -0.4444 -0.4211 -0.3871
Washington -0.2963 -0.3333 -0.4444 -0.4286 -0.3750

lost/gained NOSC


aromatic peaks


FTICR Soil – tables

relative abundance

site Class baseline drought field moist flood time zero saturation
Alaska AminoSugar 5.46 ± 0.16 4.06 ± 0.11 * 4.63 ± 0.1 * 5.66 ± 0.11 5.53 ± 0.15
Alaska Carb 6.16 ± 0.16 4.57 ± 0.06 * 5.53 ± 0.1 * 6.64 ± 0.12 * 6.72 ± 0.12
Alaska Lipid 9.3 ± 0.34 9.8 ± 0.17 11.16 ± 0.23 * 12.22 ± 0.2 * 11.43 ± 0.28
Alaska Protein 14.68 ± 0.24 13.48 ± 0.19 * 14 ± 0.13 15.67 ± 0.17 * 15.44 ± 0.3
Alaska UnsatHC 4.1 ± 0.27 5.4 ± 0.17 * 5.2 ± 0.08 * 4.89 ± 0.07 * 4.82 ± 0.04
Alaska ConHC 14.62 ± 0.43 16.89 ± 0.38 * 15.51 ± 0.1 12.99 ± 0.23 * 13.8 ± 0.26
Alaska Lignin 34.91 ± 0.48 35.65 ± 0.18 34.32 ± 0.32 32.26 ± 0.23 * 32.77 ± 0.32
Alaska Tannin 6.91 ± 0.29 6.24 ± 0.08 * 5.69 ± 0.08 * 5.86 ± 0.12 * 5.84 ± 0.1
Alaska Unnamed 3.84 ± 0.11 3.91 ± 0.05 3.96 ± 0.02 3.81 ± 0.07 3.65 ± 0.1
Florida AminoSugar 7.31 ± 0.12 4.1 ± 0.07 * 4.7 ± 0.05 * 4.08 ± 0.09 * 5.21 ± 0.15
Florida Carb 9.92 ± 0.05 4.64 ± 0.07 * 6.07 ± 0.08 * 5.51 ± 0.12 * 6.92 ± 0.12
Florida Lipid 9.31 ± 0.08 13.72 ± 0.22 * 13.65 ± 0.09 * 13.85 ± 0.3 * 12.05 ± 0.47
Florida Protein 14.49 ± 0.11 16.29 ± 0.19 * 16.48 ± 0.14 * 13.77 ± 0.16 * 14.04 ± 0.06
Florida UnsatHC 4.19 ± 0.03 5.58 ± 0.05 * 4.75 ± 0.05 * 6.23 ± 0.07 * 5.47 ± 0.16
Florida ConHC 12.17 ± 0.22 16.38 ± 0.09 * 15.19 ± 0.23 * 16.71 ± 0.3 * 15.82 ± 0.12
Florida Lignin 31.74 ± 0.17 31.48 ± 0.19 31.57 ± 0.19 31.03 ± 0.25 31.49 ± 0.32
Florida Tannin 7.03 ± 0.05 4.07 ± 0.09 * 4.15 ± 0.11 * 4.91 ± 0.1 * 5.11 ± 0.15
Florida Unnamed 3.84 ± 0.04 3.74 ± 0.07 3.44 ± 0.1 * 3.91 ± 0.07 3.89 ± 0.04
Washington AminoSugar 3.41 ± 0.13 4.64 ± 0.08 * 5.26 ± 0.22 * 5.13 ± 0.11 * 4.18 ± 0.06
Washington Carb 5.33 ± 0.03 5.48 ± 0.11 6.56 ± 0.45 * 6.63 ± 0.38 * 4.94 ± 0.19
Washington Lipid 12.02 ± 0.23 10.06 ± 0.26 * 12.78 ± 0.21 12.45 ± 0.15 12.79 ± 0.17
Washington Protein 12.17 ± 0.47 14 ± 0.39 * 14.93 ± 0.48 * 15.35 ± 0.19 * 14.15 ± 0.2
Washington UnsatHC 5.76 ± 0.13 5.37 ± 0.13 6.32 ± 0.13 * 6.16 ± 0.1 6.61 ± 0.11
Washington ConHC 20.77 ± 0.76 17.19 ± 0.19 * 12.84 ± 0.89 * 13.3 ± 0.48 * 17.08 ± 0.3
Washington Lignin 31.98 ± 0.26 33.9 ± 0.42 * 33.08 ± 0.16 * 32.68 ± 0.22 30.76 ± 0.31
Washington Tannin 5.24 ± 0.13 5.28 ± 0.12 4.7 ± 0.06 * 4.74 ± 0.08 * 5.1 ± 0.04
Washington Unnamed 3.32 ± 0.06 4.09 ± 0.05 * 3.53 ± 0.08 3.56 ± 0.16 4.38 ± 0.15

peaks

site Class baseline drought field moist flood time zero saturation
Alaska AminoSugar 495 431 523 587 540
Alaska Carb 554 472 603 675 655
Alaska Lipid 914 1056 1304 1353 1226
Alaska Protein 1313 1366 1528 1627 1527
Alaska UnsatHC 427 608 618 577 544
Alaska ConHC 1358 1684 1711 1379 1376
Alaska Lignin 3032 3414 3596 3237 3156
Alaska Tannin 587 603 598 585 563
Alaska Unnamed 385 428 463 436 391
Alaska total 9065 10062 10944 10456 9978
Florida AminoSugar 742 435 291 448 615
Florida Carb 994 476 369 589 774
Florida Lipid 990 1462 841 1555 1447
Florida Protein 1480 1653 982 1458 1615
Florida UnsatHC 461 632 308 716 683
Florida ConHC 1272 1649 923 1787 1839
Florida Lignin 3215 3088 1868 3191 3551
Florida Tannin 706 425 259 523 596
Florida Unnamed 406 415 223 454 486
Florida total 10266 10235 6064 10721 11606
Washington AminoSugar 247 552 625 607 427
Washington Carb 373 631 776 755 495
Washington Lipid 835 1220 1546 1505 1316
Washington Protein 836 1618 1725 1782 1406
Washington UnsatHC 410 651 767 770 687
Washington ConHC 1368 2000 1503 1621 1737
Washington Lignin 2111 3758 3702 3651 2951
Washington Tannin 362 607 536 547 510
Washington Unnamed 252 504 448 461 481
Washington total 6794 11541 11628 11699 10010
## unique pea ks
site Class drought field moist flood
Alaska AminoSugar 153 161 166
Alaska Carb 150 190 209
Alaska Lipid 513 659 674
Alaska Protein 469 484 552
Alaska UnsatHC 289 284 298
Alaska ConHC 634 650 440
Alaska Lignin 965 1012 844
Alaska Tannin 157 147 149
Alaska Unnamed 202 221 210
Florida AminoSugar 147 72 140
Florida Carb 125 71 184
Florida Lipid 734 271 832
Florida Protein 627 194 515
Florida UnsatHC 329 123 386
Florida ConHC 620 236 735
Florida Lignin 962 323 1043
Florida Tannin 151 58 189
Florida Unnamed 222 84 251
Washington AminoSugar 196 171 172
Washington Carb 211 184 168
Washington Lipid 541 690 647
Washington Protein 517 522 521
Washington UnsatHC 257 319 332
Washington ConHC 851 511 632
Washington Lignin 1110 966 964
Washington Tannin 246 147 175
Washington Unnamed 253 211 221

aromatic peaks

Shannon diversity

treatment Alaska Florida Washington
baseline 1.92 ± 0.01 1.99 ± 0 1.9 ± 0.01
drought 1.89 ± 0 * 1.91 ± 0 * 1.92 ± 0
field moist 1.92 ± 0.01 1.93 ± 0 * 1.94 ± 0 *
flood 1.96 ± 0 * 1.95 ± 0 * 1.95 ± 0 *
time zero saturation 1.95 ± 0 1.96 ± 0 1.95 ± 0

testing color palettes